Terbium-161 has emerged as a promising radioisotope for targeted radionuclide therapy (TRT) and has similar properties to the well-established TRT radioisotope lutetium-177.1 These include; 1) a relatively low energy beta emission (~154 keV) which are ideal for treatment of cancers characterised by small, metastatic lesions, 2) a half-life of approximately 7 days which is suitable for smaller molecules but ideal for larger biological vectors including proteins and antibodies, and 3) well-known lanthanoid chemistry which allows radiolabelling in high radiochemical yields and high specific activities. The key difference and potential significant advantage of terbium-161 are the presence large numbers of low energy Auger electron emissions (12-15 per decay) which have a very short sub-cellular range (~1 nm – 1 μm) and high linear energy transfer. These highly damaging electrons make terbium-161 an exceptionally promising candidates for treatment of metastatic cancer with difficult to treat micro-metastases.2 In addition to producing established terbium-161 radiopharmaceuticals, we are also radiolabelling new vectors including small molecules targeting glioblastoma multiforme - a highly aggressive brain cancer with low survival rates (5-7% after 5 years).3 The effectiveness of all new Tb-161 radiolabelled vectors will be evaluated in cell uptake and cell viability assays. This work is part of the ARC funded Industrial Transformation Training Centre (ITTC) for Advanced Radiochemical Technologies - a training centre that brings to ANSTO many Australian PhD students and post-doctoral researchers to train in aspects of radioisotope production, radiolabelling optimisation and radiopharmaceutical formulation and delivery.